Microwave-assisted hydrothermal synthesis of coralloid nanostructured nickel hydroxide hydrate and thermal conversion to nickel oxide

Teh Long Lai; Yuan Lung Lai; Jen Wei Yu; Youn Yuen Shu; Chen Bin Wang

doi:10.1016/j.materresbull.2009.04.017

Microwave-assisted hydrothermal synthesis of coralloid nanostructured nickel hydroxide hydrate and thermal conversion to nickel oxide

Teh Long Lai, Yuan Lung Lai, Jen Wei Yu, Youn Yuen Shu, Chen Bin Wang

工業教育與技術學系

研究成果: Article

29 引文斯高帕斯（Scopus）

摘要

Coralloid nanostructured nickel hydroxide hydrate has been successfully synthesized by a simple microwave-assisted hydrothermal process using nickel sulfate hexahydrate as precursor and urea as hydrolysis-controlling agent. A pure coralloid nanostructured nickel oxide can be obtained from the nickel hydroxide hydrate after calcination at 400 °C. The thermal property, structure and morphology of samples were characterized by thermogravimetry (TG), temperature-programmed reduction (TPR), X-ray (XRD), infrared spectroscopy (IR), scanning electron microscopy (SEM) and transmission electron microscopy (TEM).

原文	English
頁（從 - 到）	2040-2044
頁數	5
期刊	Materials Research Bulletin
卷	44
發行號	10
DOIs	https://doi.org/10.1016/j.materresbull.2009.04.017
出版狀態	Published - 2009 十月 1

All Science Journal Classification (ASJC) codes

Materials Science(all)
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

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10.1016/j.materresbull.2009.04.017

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引用此

Lai, T. L., Lai, Y. L., Yu, J. W., Shu, Y. Y., & Wang, C. B. (2009). Microwave-assisted hydrothermal synthesis of coralloid nanostructured nickel hydroxide hydrate and thermal conversion to nickel oxide. Materials Research Bulletin, 44(10), 2040-2044. https://doi.org/10.1016/j.materresbull.2009.04.017

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