Synthesis and characterization of spiral carbon nanofibers containing Pd metal cluster by using Pd2(dba)3 as catalyst

C. J. Su; L. S. Hsu; T. W. Wu; Chia-Jyi Liu; S. H. Lin

Synthesis and characterization of spiral carbon nanofibers containing Pd metal cluster by using Pd₂(dba)₃ as catalyst

C. J. Su, L. S. Hsu, T. W. Wu, Chia-Jyi Liu, S. H. Lin

Department of Physics

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

1 Citation (Scopus)

Abstract

The spiral carbon nanofibers consisting of Pd metal cluster were grown by the Pd₂(dba)₃-catalyzed decomposition of gaseous acetylene on molecular sieves (Linde 13X) support. The phase and composition of the sample was measured with x-ray diffraction (XRD). The microstructure and composition of the spiral carbon nanofibers were characterized by transmission electron microscope (TEM) and selective area diffraction (SAD). These Pd metal clusters show a small hysteresis from magnetization (M) vs. magnetic field (H) data and insulating behavior from electrical resistivity measurement. The thermopower (S) data shows metallic behavior from Pd cluster. This is the first report of incorporation of Pd nanoparticles inside carbon nanofibers.

Original language	English
Title of host publication	2003 Nanotechnology Conference and Trade Show - Nanotech 2003
Editors	M. Laudon, B. Romanowicz
Pages	13-16
Number of pages	4
Volume	3
Publication status	Published - 2003 Dec 1
Event	2003 Nanotechnology Conference and Trade Show - Nanotech 2003 - San Francisco, CA, United States Duration: 2003 Feb 23 → 2003 Feb 27

Other

Other	2003 Nanotechnology Conference and Trade Show - Nanotech 2003
Country	United States
City	San Francisco, CA
Period	03-02-23 → 03-02-27

All Science Journal Classification (ASJC) codes

Engineering(all)

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title = "Synthesis and characterization of spiral carbon nanofibers containing Pd metal cluster by using Pd2(dba)3 as catalyst",

abstract = "The spiral carbon nanofibers consisting of Pd metal cluster were grown by the Pd2(dba)3-catalyzed decomposition of gaseous acetylene on molecular sieves (Linde 13X) support. The phase and composition of the sample was measured with x-ray diffraction (XRD). The microstructure and composition of the spiral carbon nanofibers were characterized by transmission electron microscope (TEM) and selective area diffraction (SAD). These Pd metal clusters show a small hysteresis from magnetization (M) vs. magnetic field (H) data and insulating behavior from electrical resistivity measurement. The thermopower (S) data shows metallic behavior from Pd cluster. This is the first report of incorporation of Pd nanoparticles inside carbon nanofibers.",

author = "Su, {C. J.} and Hsu, {L. S.} and Wu, {T. W.} and Chia-Jyi Liu and Lin, {S. H.}",

year = "2003",

month = dec,

day = "1",

language = "English",

isbn = "0972842209",

volume = "3",

pages = "13--16",

editor = "M. Laudon and B. Romanowicz",

booktitle = "2003 Nanotechnology Conference and Trade Show - Nanotech 2003",

note = "2003 Nanotechnology Conference and Trade Show - Nanotech 2003 ; Conference date: 23-02-2003 Through 27-02-2003",

}

Su, CJ, Hsu, LS, Wu, TW, Liu, C-J & Lin, SH 2003, Synthesis and characterization of spiral carbon nanofibers containing Pd metal cluster by using Pd₂(dba)₃ as catalyst. in M Laudon & B Romanowicz (eds), 2003 Nanotechnology Conference and Trade Show - Nanotech 2003. vol. 3, pp. 13-16, 2003 Nanotechnology Conference and Trade Show - Nanotech 2003, San Francisco, CA, United States, 03-02-23.

Synthesis and characterization of spiral carbon nanofibers containing Pd metal cluster by using Pd₂(dba)₃ as catalyst. / Su, C. J.; Hsu, L. S.; Wu, T. W.; Liu, Chia-Jyi; Lin, S. H.

2003 Nanotechnology Conference and Trade Show - Nanotech 2003. ed. / M. Laudon; B. Romanowicz. Vol. 3 2003. p. 13-16.

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

TY - GEN

T1 - Synthesis and characterization of spiral carbon nanofibers containing Pd metal cluster by using Pd2(dba)3 as catalyst

AU - Su, C. J.

AU - Hsu, L. S.

AU - Wu, T. W.

AU - Liu, Chia-Jyi

AU - Lin, S. H.

PY - 2003/12/1

Y1 - 2003/12/1

N2 - The spiral carbon nanofibers consisting of Pd metal cluster were grown by the Pd2(dba)3-catalyzed decomposition of gaseous acetylene on molecular sieves (Linde 13X) support. The phase and composition of the sample was measured with x-ray diffraction (XRD). The microstructure and composition of the spiral carbon nanofibers were characterized by transmission electron microscope (TEM) and selective area diffraction (SAD). These Pd metal clusters show a small hysteresis from magnetization (M) vs. magnetic field (H) data and insulating behavior from electrical resistivity measurement. The thermopower (S) data shows metallic behavior from Pd cluster. This is the first report of incorporation of Pd nanoparticles inside carbon nanofibers.

AB - The spiral carbon nanofibers consisting of Pd metal cluster were grown by the Pd2(dba)3-catalyzed decomposition of gaseous acetylene on molecular sieves (Linde 13X) support. The phase and composition of the sample was measured with x-ray diffraction (XRD). The microstructure and composition of the spiral carbon nanofibers were characterized by transmission electron microscope (TEM) and selective area diffraction (SAD). These Pd metal clusters show a small hysteresis from magnetization (M) vs. magnetic field (H) data and insulating behavior from electrical resistivity measurement. The thermopower (S) data shows metallic behavior from Pd cluster. This is the first report of incorporation of Pd nanoparticles inside carbon nanofibers.

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M3 - Conference contribution

AN - SCOPUS:6344258313

SN - 0972842209

VL - 3

SP - 13

EP - 16

BT - 2003 Nanotechnology Conference and Trade Show - Nanotech 2003

A2 - Laudon, M.

A2 - Romanowicz, B.

T2 - 2003 Nanotechnology Conference and Trade Show - Nanotech 2003

Y2 - 23 February 2003 through 27 February 2003

ER -