Abstract
Coralloid nanostructured nickel hydroxide hydrate has been successfully synthesized by a simple microwave-assisted hydrothermal process using nickel sulfate hexahydrate as precursor and urea as hydrolysis-controlling agent. A pure coralloid nanostructured nickel oxide can be obtained from the nickel hydroxide hydrate after calcination at 400 °C. The thermal property, structure and morphology of samples were characterized by thermogravimetry (TG), temperature-programmed reduction (TPR), X-ray (XRD), infrared spectroscopy (IR), scanning electron microscopy (SEM) and transmission electron microscopy (TEM).
| Original language | English |
|---|---|
| Pages (from-to) | 2040-2044 |
| Number of pages | 5 |
| Journal | Materials Research Bulletin |
| Volume | 44 |
| Issue number | 10 |
| DOIs | |
| Publication status | Published - 2009 Oct 1 |
All Science Journal Classification (ASJC) codes
- Materials Science(all)
- Condensed Matter Physics
- Mechanics of Materials
- Mechanical Engineering
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Cite this
Lai, T. L., Lai, Y. L., Yu, J. W., Shu, Y. Y., & Wang, C. B. (2009). Microwave-assisted hydrothermal synthesis of coralloid nanostructured nickel hydroxide hydrate and thermal conversion to nickel oxide. Materials Research Bulletin, 44(10), 2040-2044. https://doi.org/10.1016/j.materresbull.2009.04.017