Abstract
Coralloid nanostructured nickel hydroxide hydrate has been successfully synthesized by a simple microwave-assisted hydrothermal process using nickel sulfate hexahydrate as precursor and urea as hydrolysis-controlling agent. A pure coralloid nanostructured nickel oxide can be obtained from the nickel hydroxide hydrate after calcination at 400 °C. The thermal property, structure and morphology of samples were characterized by thermogravimetry (TG), temperature-programmed reduction (TPR), X-ray (XRD), infrared spectroscopy (IR), scanning electron microscopy (SEM) and transmission electron microscopy (TEM).
| Original language | English |
|---|---|
| Pages (from-to) | 2040-2044 |
| Number of pages | 5 |
| Journal | Materials Research Bulletin |
| Volume | 44 |
| Issue number | 10 |
| DOIs | |
| Publication status | Published - 2009 Oct 1 |
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All Science Journal Classification (ASJC) codes
- Materials Science(all)
- Condensed Matter Physics
- Mechanical Engineering
- Mechanics of Materials
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Microwave-assisted hydrothermal synthesis of coralloid nanostructured nickel hydroxide hydrate and thermal conversion to nickel oxide. / Lai, Teh Long; Lai, Yuan-Lung; Yu, Jen Wei; Shu, Youn Yuen; Wang, Chen Bin.
In: Materials Research Bulletin, Vol. 44, No. 10, 01.10.2009, p. 2040-2044.Research output: Contribution to journal › Article
TY - JOUR
T1 - Microwave-assisted hydrothermal synthesis of coralloid nanostructured nickel hydroxide hydrate and thermal conversion to nickel oxide
AU - Lai, Teh Long
AU - Lai, Yuan-Lung
AU - Yu, Jen Wei
AU - Shu, Youn Yuen
AU - Wang, Chen Bin
PY - 2009/10/1
Y1 - 2009/10/1
N2 - Coralloid nanostructured nickel hydroxide hydrate has been successfully synthesized by a simple microwave-assisted hydrothermal process using nickel sulfate hexahydrate as precursor and urea as hydrolysis-controlling agent. A pure coralloid nanostructured nickel oxide can be obtained from the nickel hydroxide hydrate after calcination at 400 °C. The thermal property, structure and morphology of samples were characterized by thermogravimetry (TG), temperature-programmed reduction (TPR), X-ray (XRD), infrared spectroscopy (IR), scanning electron microscopy (SEM) and transmission electron microscopy (TEM).
AB - Coralloid nanostructured nickel hydroxide hydrate has been successfully synthesized by a simple microwave-assisted hydrothermal process using nickel sulfate hexahydrate as precursor and urea as hydrolysis-controlling agent. A pure coralloid nanostructured nickel oxide can be obtained from the nickel hydroxide hydrate after calcination at 400 °C. The thermal property, structure and morphology of samples were characterized by thermogravimetry (TG), temperature-programmed reduction (TPR), X-ray (XRD), infrared spectroscopy (IR), scanning electron microscopy (SEM) and transmission electron microscopy (TEM).
UR - http://www.scopus.com/inward/record.url?scp=68749083588&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=68749083588&partnerID=8YFLogxK
U2 - 10.1016/j.materresbull.2009.04.017
DO - 10.1016/j.materresbull.2009.04.017
M3 - Article
AN - SCOPUS:68749083588
VL - 44
SP - 2040
EP - 2044
JO - Materials Research Bulletin
JF - Materials Research Bulletin
SN - 0025-5408
IS - 10
ER -